反应条件
magnesium; ethylene dibromide in tetrahydrofuran
inert atmosphere, activation of Mg with ethylene bromide in THF, addn. of THF and a further portion of ethylene bromide, reflux, addn. of soln. of dibromobenzene and soln. of (CH3)3SnCl to the boiling soln., reflux (6 h); saturated aq. NH4Cl, extn. (Et2O), washing of extracts (water), drying (Na2SO4), concn. (reduced pressure), distillation (90-94°C, 0.1 Torr or 92-94°C, 0.145 Torr);
参考文献
Eisch, John J.; Kotowicz, Boguslaw W.
European Journal of Inorganic Chemistry, 1998 , # 6 p. 761 - 769
