Qadir, Maryiam; Priestley, Rachael E.; Rising, Thomas W. D. F.; Gelbrich, Thomas; Coles, Simon J.; Hursthouse, Michael B.; Sheldrake, Peter W.; Whittall, Neil; Hii
Tetrahedron Letters, 2003 , vol. 44, # 18 p. 3675 - 3678
1.1: Mg / tetrahydrofuran
1.2: tetrahydrofuran / 14 h / 20 °C
1.3: 40 percent / iodine / tetrahydrofuran / 0.5 h / 20 °C
2.1: 98 percent / BBr3 / CH2Cl2 / -78 - 20 °C
3.1: 46 percent / Cu(OAc)2; triethylamine; oxygen / CH2Cl2 / 48 h / 20 °C / 760 Torr
4.1: 89 percent / 1,1-bis(diphenylphosphino)methane; CsO2CCMe3; Pd(OAc)2 / dimethylformamide / 24 h / 110 °C
View Scheme
参考文献
Campo, Marino A.; Huang, Qinhua; Yao, Tuanli; Tian, Qingping; Larock, Richard C.
Journal of the American Chemical Society, 2003 , vol. 125, # 38 p. 11506 - 11507