1: With trimethylsilylating agent
2: With 4-methoxypyridine-N-oxide; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione in dichloromethane; dimethyl sulfoxide
T=20°C; 1 h; Title compound not separated from byproducts;
参考文献
Nicolaou; Gray, David L. F.; Montagnon, Tamsyn; Harrison, Scott T.
Angewandte Chemie - International Edition, 2002 , vol. 41, # 6 p. 996 - 1000
Kishan, M. Radha; Srinivas; Kulkarni; Raghavan
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2002 , vol. 41, # 5 p. 1075 - 1077
Smith, John R. Lindsay; Thomas, C. Barry; Whittaker, Mark
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1993 , # 11 p. 2191 - 2194
chloro-trimethyl-silane; triethylamine
1) DMF, reflux 2) THF a) -38 deg C, 1.4 h b) -38 to 10 deg C, 3.7 h c) r.t., 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Chen, Kuanchiang; Koser, Gerald F.
Journal of Organic Chemistry, 1991 , vol. 56, # 20 p. 5764 - 5767
