反应条件
1.1: m-nitrobenzene sulfonic acid sodium salt; iron sulphate heptahydrate / methanesulfonic acid / 118 - 125 °C / |Large scale 1.2: 125 - 133 °C / |Large scale 2.1: VAZO-52; N-bromosuccinmide / chlorobenzene / 19 h / 48 - 52 °C / |Inert atmosphere; |Large scale 3.1: N,N-dimethyl-formamide / 3 h / 13 - 17 °C / |Large scale 3.2: 1 h / 75 - 80 °C / |Large scale 4.1: sodium t-butanolate / N,N-dimethyl-formamide 5.1: sodium t-butanolate / N,N-dimethyl-formamide View Scheme
参考文献
Conlon, David A.; Drahus-Paone, Antoinette; Ho, Guo-Jie; Pipik, Brenda; Helmy, Roy; McNamara, James M.; Shi, Yao-Jun; Williams, J. Michael; Macdonald, Dwight; Deschenes, Denis; Gallant, Michel; Mastracchio, Anthony; Roy, Bruno; Scheigetz, John
Organic Process Research and Development, 2006 , vol. 10, # 1 p. 36 - 45
