反应条件
1.1: magnesium / tetrahydrofuran / 2 h / 20 - 85 °C
1.2: 0 - 20 °C / |Inert atmosphere
2.1: pyridinium chlorochromate; triethylamine / dichloromethane / 20 °C
3.1: palladium diacetate; trifluoroacetic acid; potassium carbonate; silver(l) oxide / 24 h / 140 °C / |Schlenk technique; |Inert atmosphere
View Scheme
参考文献
Li, Hu; Zhu, Ru-Yi; Shi, Wen-Juan; He, Ke-Han; Shi, Zhang-Jie
Organic Letters, 2012 , vol. 14, # 18 p. 4850 - 4853,4