N,N-二甲基氢化肉桂酰胺合成路线 （共 32 条）
反应条件
1: With 1,3-bis-(diphenylphosphino)propane; caesium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in toluene
T=150°C; 72 h;
2: With hydrogen; palladium on activated charcoal in diethyl ether
P=760 Torr; 12 h;
参考文献
Black, Phillip J.; Edwards, Michael G.; Williams, Jonathan M. J.
European Journal of Organic Chemistry, 2006 , # 19 p. 4367 - 4378
反应条件
sodium cyanide in methanol
T=50°C; 78 h;
参考文献
Hoegberg, Thomas; Stroem, Peter; Ebner, Michael; Raemsby, Sten
Journal of Organic Chemistry, 1987 , vol. 52, # 10 p. 2033 - 2036
反应条件
sodium hydroxide in tetrahydrofuran
T=25°C; 6 h;
参考文献
Hall, Larry R.; Iwamoto, Reynold T.; Hanzlik, Robert P.
Journal of Organic Chemistry, 1989 , vol. 54, # 10 p. 2446 - 2451
反应条件
sulfuryl dichloride
T=40 - 90°C; 1.75 h;
参考文献
Ward, Robert S.; Davies, Joanna; Hodges, Geoffrey; Roberts, David W.
Synthesis, 2002 , # 16 p. 2431 - 2439
反应条件
palladium diacetate; potassium carbonate; dicyclohexyl(2',6'-diisopropoxy-[1,1'-biphenyl]-2-yl)phosphine in water; toluene
T=85°C; Suzuki-Miyaura coupling; 14 h; Inert atmosphere;
参考文献
Molander, Gary A.; Jean-Gerard, Ludivine
Journal of Organic Chemistry, 2009 , vol. 74, # 15 p. 5446 - 5450
反应条件
1,1'-bis-(diphenylphosphino)ferrocene in water; toluene
T=80°C; 10 h; Heating;
参考文献
Zou, Gang; Guo, Jianping; Wang, Zhiyong; Huang, Wen; Tang, Jie
Dalton Transactions, 2007 , # 28 p. 3055 - 3064
反应条件
C29H55IrN3P2(1+)*Cl(1-); potassium tert-butylate in toluene
T=120°C; 15 h; Schlenk techniqueInert atmosphereGlovebox; SolventReagent/catalyst;
参考文献
Guo, Le; Liu, Yinghua; Yao, Wubing; Leng, Xuebing; Huang, Zheng
Organic Letters, 2013 , vol. 15, # 5 p. 1144 - 1147
反应条件
p-toluenesulfinyl chloride; N-ethyl-N,N-diisopropylamine in dichloromethane
参考文献
Magnus, Philip; Pappalardo, Paul A.
Journal of the American Chemical Society, 1986 , vol. 108, # 2 p. 212 - 217
反应条件
1,3-bis-(diphenylphosphino)propane; caesium carbonate; di-μ-chloro-bis(η4-1,5-cyclooctadiene)diiridium in toluene
T=150°C; 72 h; Title compound not separated from byproducts;
参考文献
Black, Phillip J.; Edwards, Michael G.; Williams, Jonathan M. J.
European Journal of Organic Chemistry, 2006 , # 19 p. 4367 - 4378
反应条件
1,1'-carbonyldiimidazole
T=160 - 165°C; 0.5 h;
参考文献
Aavula, Sanjeev Kumar; Chikkulapally, Anil; Hanumanthappa; Jyothi, Indira; Vinod; Sulur, Kumar; Manjunatha; Sythana, Suresh Kumar
Journal of Chemical Research, 2013 , vol. 37, # 3 p. 155 - 159
