1-苄基-4-氯-1,8-萘啶-2(1h)-酮合成路线 （共 7 条）
反应条件
caesium carbonate; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane Suzuki coupling reaction; 4 h; Heating;
参考文献
Ban, Hitoshi; Muraoka, Masami; Ohashi, Naohito
Tetrahedron, 2005 , vol. 61, # 42 p. 10081 - 10092
反应条件
trichlorophosphate
2 h; Heating / reflux;
参考文献
Yang, Zhen; Fathi, Reza; Zhu, Qiang; Cho, Hyun-Joon; Liu, Yixin; Sandrasagra, Anthony; Wobbe, C. Richard
Patent: US2009/54477 A1, 2009 ;
Location in patent: Page/Page column 18 ;
US 20090054477 A1
反应条件
trichlorophosphate
T=90°C;
参考文献
Ban, Hitoshi; Muraoka, Masami; Ohashi, Naohito
Tetrahedron, 2005 , vol. 61, # 42 p. 10081 - 10092
反应条件
1: 71 percent / 10 h / 90 °C
2: 63 percent / acetic acid / 2 h / Heating
3: 100 percent / K2CO3; water / methanol / 3 h / 20 °C
4: 84 percent / POCl3 / 0.5 h / 90 °C
View Scheme
参考文献
Ban, Hitoshi; Muraoka, Masami; Ohashi, Naohito
Tetrahedron, 2005 , vol. 61, # 42 p. 10081 - 10092
反应条件
1: 63 percent / acetic acid / 2 h / Heating
2: 100 percent / K2CO3; water / methanol / 3 h / 20 °C
3: 84 percent / POCl3 / 0.5 h / 90 °C
View Scheme
参考文献
Ban, Hitoshi; Muraoka, Masami; Ohashi, Naohito
Tetrahedron, 2005 , vol. 61, # 42 p. 10081 - 10092
反应条件
1: 100 percent / K2CO3; water / methanol / 3 h / 20 °C
2: 84 percent / POCl3 / 0.5 h / 90 °C
View Scheme
参考文献
Ban, Hitoshi; Muraoka, Masami; Ohashi, Naohito
Tetrahedron, 2005 , vol. 61, # 42 p. 10081 - 10092
反应条件
1: 71 percent / 10 h / 90 °C
2: 63 percent / acetic acid / 2 h / Heating
3: 100 percent / K2CO3; water / methanol / 3 h / 20 °C
4: 84 percent / POCl3 / 0.5 h / 90 °C
View Scheme
参考文献
Ban, Hitoshi; Muraoka, Masami; Ohashi, Naohito
Tetrahedron, 2005 , vol. 61, # 42 p. 10081 - 10092
