2-巯基-4,6-二苯基-烟腈合成路线 （共 13 条）
反应条件
1: 50 percent / Br2 / CHCl3 / 20 h / 0 °C 2: 37 percent / Br2 / CHCl3 / 2 h / 20 °C View Scheme
参考文献
Krauze, A. A.; Bomika, Z. A.; Pelcher, Yu. E.; Mazheika, I. B.; Dubur, G. Ya.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 4 p. 385 - 390
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 4 p. 508 - 512
反应条件
potassium hydroxide in N,N-dimethyl-formamide
T=15 - 20°C; 0.5 h;
参考文献
Krauze, A. A.; Bomika, Z. A.; Shestopalov, A. M.; Rodinovskaya, L. A.; Pelcher, Yu. E'; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 3 p. 279 - 284
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 3 p. 377 - 382
反应条件
potassium hydroxide in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Shestopalov, A. M.; Promonenkov, V. K.; Sharanin, Yu. A.; Rodinovskaya, L. A.; Sharanin, S. Yu.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 7 p. 1382 - 1401
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 7 p. 1517 - 1538
反应条件
sodium methylate in methanol
1 h; Heating;
参考文献
Krauze, A. A.; Bomika, Z. A.; Shestopalov, A. M.; Rodinovskaya, L. A.; Pelcher, Yu. E'; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 3 p. 279 - 284
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 3 p. 377 - 382
反应条件
sodium ethanolate in ethanol
0.25 h; Heating;
参考文献
Wagner; Leistner; Vieweg; Krasselt; Prantz
Pharmazie, 1993 , vol. 48, # 7 p. 514 - 518
反应条件
potassium hydroxide in N,N-dimethyl-formamide
Ambient temperature;
参考文献
Shestopalov, A. M.; Promonenkov, V. K.; Sharanin, Yu. A.; Rodinovskaya, L. A.; Sharanin, S. Yu.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, # 7 p. 1382 - 1401
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 7 p. 1517 - 1538
反应条件
1: 70 percent / 10percent aq. KOH / dimethylformamide / Ambient temperature
2: 10percent aq. KOH / dimethylformamide
View Scheme
参考文献
Shestopalov, A. M.; Sharanin, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1984 , p. 1818 - 1827
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 9 p. 1991 - 2002
反应条件
potassium hydroxide in N,N-dimethyl-formamide
T=15 - 20°C; 0.5 h;
参考文献
Krauze, A. A.; Bomika, Z. A.; Shestopalov, A. M.; Rodinovskaya, L. A.; Pelcher, Yu. E'; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 3 p. 279 - 284
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 3 p. 377 - 382
反应条件
sodium methylate in methanol
0.166667 h; Heating;
参考文献
Wagner; Leistner; Vieweg; Krasselt; Prantz
Pharmazie, 1993 , vol. 48, # 7 p. 514 - 518
反应条件
1: TEA / ethanol / 0.17 h / Heating
2: NaOEt / ethanol / 0.08 h / Heating
View Scheme
参考文献
Krauze, A. A.; Bomika, Z. A.; Shestopalov, A. M.; Rodinovskaya, L. A.; Pelcher, Yu. E'; et al.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1981 , vol. 17, # 3 p. 279 - 284
Khimiya Geterotsiklicheskikh Soedinenii, 1981 , vol. 17, # 3 p. 377 - 382
