hydrogen; palladium on activated charcoal in ethanol T=20°C; 0.0833333 h; the formed intermediates are separated with gas chromatography and detected with 1H-NMR-spectroscopy after several times; Product distribution;
参考文献
Hertzsch, Winfried; Musso, Hans
Liebigs Annalen der Chemie, 1985 , # 7 p. 1485 - 1491
1: With hydrogen; N-heterocyclic carbene complex in dichloromethane T=25°C; P=15201 Torr; 4 h; 2: With lithium aluminium tetrahydride Further stages. Title compound not separated from byproducts.;
参考文献
Zhou, Jianguang; Ogle, James W.; Fan, Yubo; Banphavichit, Yorawit; Zhu, Ye; Burgess, Kevin
Chemistry - A European Journal, 2007 , vol. 13, # 25 p. 7162 - 7170
1: With hydrogen; N-heterocyclic carbene complex in dichloromethane T=25°C; P=15201 Torr; 4 h; 2: With lithium aluminium tetrahydride Further stages. Title compound not separated from byproducts.;
参考文献
Zhou, Jianguang; Ogle, James W.; Fan, Yubo; Banphavichit, Yorawit; Zhu, Ye; Burgess, Kevin
Chemistry - A European Journal, 2007 , vol. 13, # 25 p. 7162 - 7170
aluminium trichloride in dichloromethane 3.5 h; Irradiation;
参考文献
Lewis, Frederick D.; Howard, Daniel K.; Barancyk, Steven V.; Oxman, Joe D.
Journal of the American Chemical Society, 1986 , vol. 108, # 11 p. 3016 - 3023