反应条件
1: 99 percent / polystyrene-supported chlorite; polystyrene-supported dihydrogenphosphate; 2,3-dimethylbutene / 2-methyl-propan-2-ol; H2O; tetrahydrofuran / 6 h / 20 °C
2: 100 percent / TBAF / tetrahydrofuran / 4 h / 20 °C
3: Et3N / tetrahydrofuran / 0.83 h / 20 °C
4: polystyrene-supported DMAP / toluene / 2 h / 80 °C
5: 2.2 mg / polymer-supported TsOH / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Storer, R. Ian; Takemoto, Toshiyasu; Jackson, Philip S.; Brown, Dearg S.; Baxendale, Ian R.; Ley, Steven V.
Chemistry - A European Journal, 2004 , vol. 10, # 10 p. 2529 - 2547
