1-溴-2,4-二硝基苯合成路线 (共 145 条)
反应条件
1: dimethylformamide 2: KF / dimethylformamide 3: SnCl2, HCl / diethyl ether 4: NaNO2, H2SO4 / H2O 5: H2O / Heating View Scheme
参考文献
Molecular crystals and liquid crystals, , vol. 109, # 2-4 p. 169 - 178
反应条件
(i) PhLi, (ii) /BRN= 1900390/; Multistep reaction;
参考文献
Buck,P.; Koebrich,G.
Chemische Berichte, 1970 , vol. 103, p. 1420 - 1430
反应条件
tetrabutyl ammonium fluoride T=20°C; 2 h;
参考文献
Bram, Georges; Loupy, Andre; Pigeon, Philippe
Synthetic Communications, 1988 , vol. 18, # 14 p. 1661 - 1668
反应条件
1: dimethylformamide 2: KF / dimethylformamide 3: SnCl2, HCl / diethyl ether View Scheme
参考文献
Sasaki; Takeuchi; Sato; Takatsu
Molecular crystals and liquid crystals, 1984 , vol. 109, # 2-4 p. 169 - 178
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Blanksma; van den Broek; Hoegen
Recueil des Travaux Chimiques des Pays-Bas, 1946 , vol. 65, p. 329,330
参考文献
Woroshzow; Jakobson
Zhurnal Obshchei Khimii, 1957 , vol. 27, p. 1672,1674; engl. Ausg. S. 1741, 1743
参考文献
Schoepff
Chemische Berichte, 1889 , vol. 22, p. 900
反应条件
in acetonitrile T=25°C; Kinetics; Solvent;
参考文献
Um, Ik-Hwan; Im, Li-Ra; Kang, Ji-Sun; Bursey, Samantha S.; Dust, Julian M.
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9738 - 9746
参考文献
van Romburgh
Recueil des Travaux Chimiques des Pays-Bas, 1885 , vol. 4, p. 191
反应条件
potassium carbonate in N,N-dimethyl-formamide T=55°C; 12 h;
参考文献
Sandbhor, Mahendra S.; Key, Jessie A.; Strelkov, Ileana S.; Cairo, Christopher W.
Journal of Organic Chemistry, 2009 , vol. 74, # 22 p. 8669 - 8674