2-烯丙基-4-甲氧基苯酚合成路线 (共 28 条)
反应条件
T=185°C; sowie 197grad; Rate constant;
参考文献
Goering; Jacobson
Journal of the American Chemical Society, 1958 , vol. 80, p. 3277,3279
反应条件
T=160°C; sowie 181grad und 200grad; Rate constant;
参考文献
White et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 3271,3272
参考文献
Mauthner
Journal fuer Praktische Chemie (Leipzig), 1921 , vol. <2> 102, p. 42
反应条件
ammonium cerium(IV) nitrate in acetonitrile
T=0°C; 0.75 h;
参考文献
Mehta, Goverdhan; Pan, Subhas Chandra
Organic Letters, 2004 , vol. 6, # 22 p. 3985 - 3988
反应条件
1: K2CO3 / acetone / Heating
2: 1.) OsO4, 2.) sodium metaperiodate / 1.) THF, water, 0 deg C, 1 h, 2.) 0 deg C, 0.5 h; room temperature, 3 h
3: 56 percent / toluene-p-sulfonic acid / 1,2-dimethoxy-ethane / 30 h / Heating
4: 67 percent / BBr3 / CH2Cl2 / 1.) -78 deg C, 1 h, 2.) -78 deg C to room temperature, 1 h, 3.) room temperature, 1.5 h
View Scheme
参考文献
Deshmukh, M. N.; Joshi, Shreerang V.
Synthetic Communications, 1988 , vol. 18, # 13 p. 1483 - 1490
反应条件
1: 48 percent / conc. H2SO4 / acetic acid / 20 h / Heating
2: 1.) POCl3 / 1.) RT, 30 min, 2.) 65 deg C, 3 h
View Scheme
参考文献
Nichols, David E.; Hoffman, Andrew J.; Oberlender, Robert A.; Riggs, Robert M.
Journal of Medicinal Chemistry, 1986 , vol. 29, # 2 p. 302 - 304
反应条件
1: 70 percent / KOH / methanol / 1 h / 160 °C
2: pyridine
View Scheme
参考文献
Santos, Paula M.; Figueiredo, A. Cristina; Oliveira, M. Margarida; Barroso, Jose G.; Pedro, Luis G.; Deans, Stanley G.; Younus; Scheffer, Johannes J. C.
Phytochemistry, 1998 , vol. 48, # 3 p. 455 - 460
反应条件
1: 99 percent / K2CO3 / butan-2-one / 18 h / Heating
2: 70 percent / 12 h / 190 °C
View Scheme
参考文献
Eastman Kodak Co.
Patent: US2682474 , 1951 ;