3-异丙基-1-苯基-1H-吡唑合成路线 (共 4 条)
反应条件
boron trifluoride diethyl etherate in dichloromethane
T=20°C; 4 h; Inert atmosphere; regioselective reaction;
参考文献
Shan, Gang; Liu, Pengfei; Rao, Yu
Organic Letters, 2011 , vol. 13, # 7 p. 1746 - 1749
反应条件
bis-triphenylphosphine-palladium(II) chloride; potassium tert-butylate; hydrogen in toluene
Reflux;
参考文献
Chen, Chun-Yen; Huang, Yu-Ying; Su, Wei-Nien; Kaneko, Kimiyoshi; Kimura, Masayuki; Takayama, Hiroyuki; Wong, Fung Fuh
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 1 p. 183 - 189
反应条件
1: phosphorus tribromide / acetonitrile / 20 °C / Reflux
2: bis-triphenylphosphine-palladium(II) chloride; potassium tert-butylate; hydrogen / toluene / Reflux
View Scheme
参考文献
Chen, Chun-Yen; Huang, Yu-Ying; Su, Wei-Nien; Kaneko, Kimiyoshi; Kimura, Masayuki; Takayama, Hiroyuki; Wong, Fung Fuh
Journal of Heterocyclic Chemistry, 2012 , vol. 49, # 1 p. 183 - 189
反应条件
hydroxylamine hydrochloride; sodium carbonate in ethanol
15 h; Heating; Yield given;
参考文献
Falorni, Massimo; Lardicci, Luciano; Giacomelli, Giampaolo
Gazzetta Chimica Italiana, 1987 , vol. 117, # 1 p. 7 - 10