1-[2,4-二羟基-3-[(2-羟基苯基)甲基]-6-甲氧基苯基]-3-苯基-1-丙酮合成路线 （共 19 条）
反应条件
1: 0.275 g / BF3*Et2O / dioxane / 3 h / 60 - 70 °C
2: 0.34 g / K2CO3, KI / acetone / 6 h / Heating
3: 0.22 g / aq. KOH / ethanol; dimethylsulfoxide / 24 h / Ambient temperature
4: 30 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
hydrogen; palladium on activated charcoal
参考文献
Malterud, Karl Egil; Undheim, Jorunn; Erdal, John Erik
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4807 - 4810
反应条件
hydrogen; palladium on activated charcoal
参考文献
Malterud, Karl Egil; Undheim, Jorunn; Erdal, John Erik
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4807 - 4810
反应条件
hydrogen; palladium on activated charcoal in ethyl acetate
P=760 Torr; Ambient temperature;
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 0.34 g / K2CO3, KI / acetone / 6 h / Heating
2: 0.22 g / aq. KOH / ethanol; dimethylsulfoxide / 24 h / Ambient temperature
3: 30 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 0.22 g / aq. KOH / ethanol; dimethylsulfoxide / 24 h / Ambient temperature
2: 30 mg / H2 / Pd-C (10percent) / ethyl acetate / 760 Torr / Ambient temperature
View Scheme
参考文献
Jain, Amolak C.; Arya, Prabhat
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1985 , vol. 24, p. 1015 - 1022
反应条件
1: 9 percent / KOH / H2O / 360 h / 4 °C
2: 75 percent / H2 / 10percent Pd/C
View Scheme
参考文献
Malterud, Karl Egil; Undheim, Jorunn; Erdal, John Erik
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4807 - 4810
反应条件
1: 60 percent / H2 / 10percent Pd/C
2: 9 percent / KOH / H2O / 360 h / 4 °C
3: 75 percent / H2 / 10percent Pd/C
View Scheme
参考文献
Malterud, Karl Egil; Undheim, Jorunn; Erdal, John Erik
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4807 - 4810
反应条件
1: 79 percent / KOH / H2O / 360 h / 4 °C
2: 73 percent / H2 / 10percent Pd/C
View Scheme
参考文献
Malterud, Karl Egil; Undheim, Jorunn; Erdal, John Erik
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4807 - 4810
反应条件
1: 29 percent Chromat. / AlCl3 / chlorobenzene
2: 60 percent / ethanol / 4 h / Heating
3: 60 percent / H2 / 10percent Pd/C
4: 9 percent / KOH / H2O / 360 h / 4 °C
5: 75 percent / H2 / 10percent Pd/C
View Scheme
参考文献
Malterud, Karl Egil; Undheim, Jorunn; Erdal, John Erik
Tetrahedron Letters, 1985 , vol. 26, # 39 p. 4807 - 4810
