拉凡醇; 5-甲基-2-(1-甲基乙烯基)-4-己烯-1-醇合成路线 （共 65 条）
反应条件
boron trifluoride diethyl etherate in dichloromethane; water 1 h; Ambient temperature;
参考文献
Ueno, Yoshio; Aoki, Seiichi; Okawara, Makoto
Journal of the Chemical Society, Chemical Communications, 1980 , # 15 p. 683 - 684
反应条件
lithium aluminium tetrahydride
参考文献
Calo, Vincenzo; Lopez, Luigi; Pesce, Giannangelo
Gazzetta Chimica Italiana, 1990 , vol. 120, # 3 p. 203 - 205
反应条件
2: 85 percent / sodium bis(trimethylsilyl)amide / tetrahydrofuran; toluene / 0.5 h / Heating 3: 96 percent / HCl, KF, MeOH / CH2Cl2 / 2 h / Ambient temperature 4: 59 percent / H2O2, NaHCO3, H2O / methanol; tetrahydrofuran / 12 h / Heating View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 17 p. 2701 - 2709
反应条件
1: 1.) LDA / 1.) THF, 2.) THF 2: 68 percent / aq. CuCl2 / 2.5 h / Ambient temperature 3: 66 percent / NaBH4 / ethanol / 4 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 3 p. 734 - 735
反应条件
1: 68 percent / aq. CuCl2 / 2.5 h / Ambient temperature 2: 66 percent / NaBH4 / ethanol / 4 h / Ambient temperature View Scheme
参考文献
Journal of Organic Chemistry, , vol. 62, # 3 p. 734 - 735
反应条件
1: endo,endo-3-(isopropylamino)-2-hydroxybornane / CH2Cl2 / 8 h / -40 °C / Irradiation 2: LiAlH4 / tetrahydrofuran / 2 h / 0 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 60, # 24 p. 7879 - 7883
反应条件
hexamethyl-distannane in benzene T=25°C; 5 h; Irradiation; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Chemistry Letters, , p. 1899 - 1902
反应条件
oxalic acid in water 5 h; Heating; Further byproducts given. Yields of byproduct given;
参考文献
Bertrand, M.; Waegell, B.; Zahra, J. P.
Bulletin de la Societe Chimique de France, 1991 , # 6 p. 904 - 910
反应条件
1: 95 percent / LDA / tetrahydrofuran / -78 °C 2: 63 percent / H2O, 10percent HCl / acetonitrile / 6 h / 50 °C 3: hydrure de lithium aluminium / diethyl ether / 1.5 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 40, # 9 p. 1573 - 1580
反应条件
1: 86 percent / 5percent CH3COOH / tetrahydrofuran / 16 h 2: 95 percent / LDA / tetrahydrofuran / -78 °C 3: 63 percent / H2O, 10percent HCl / acetonitrile / 6 h / 50 °C 4: hydrure de lithium aluminium / diethyl ether / 1.5 h / Ambient temperature View Scheme
参考文献
Tetrahedron, , vol. 40, # 9 p. 1573 - 1580
