拉凡醇; 5-甲基-2-(1-甲基乙烯基)-4-己烯-1-醇合成路线 （共 65 条）
反应条件
barium dihydroxide; ethanol Umsetzung mit CH3MgI, Behandlung mit Phthalsaeureanhydrid bei 150grad und anschliessende Verseifung;
参考文献
Helvetica Chimica Acta, , vol. 25, p. 1584
Helvetica Chimica Acta, , vol. 18, p. 441
反应条件
sodium hydrogen sulphate; tin(IV) chloride 2) CH2Cl2, 20 - 30 min, 0 deg C; 3) room temperature, 6 h, CH2Cl2; Yield given. Multistep reaction;
参考文献
Synthetic Communications, , vol. 11, # 4 p. 299 - 302
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine in hexane 24 h; Ambient temperature; Yields of byproduct given;
参考文献
Babin, D.; Fourneron, J. D.; Harwood, L. M.; Julia, M.
Tetrahedron, 1981 , vol. 37, p. 325 - 332
反应条件
1: K2CO3 / 1.) 45 min, RT 2.) methanol, water, RT 2: 78 percent / potassium hydrogenesulfate / 65 - 70 °C / 1 Torr / destillation View Scheme
参考文献
Bulletin de la Societe Chimique de France, , vol. 2, # 11-12 p. 588 - 600
反应条件
1: 1.) n-Bu2CuLi / 1.) THF, -30 deg C, 20 min, 2.) 30 min 2: 95 percent / LiAlH4 View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 120, # 3 p. 203 - 205
反应条件
1: 1.) n-Bu2CuLi / 1.) THF, -30 deg C, 20 min, 2.) 30 min 2: 95 percent / LiAlH4 View Scheme
参考文献
Gazzetta Chimica Italiana, , vol. 120, # 3 p. 203 - 205
参考文献
Journal of Organic Chemistry, , vol. 35, # 3 p. 790 - 793
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 47, # 47 p. 9727 - 9736
反应条件
oxalic acid 5 h; Heating; Mechanism;
参考文献
Bertrand, M.; Waegell, B.; Zahra, J. P.
Bulletin de la Societe Chimique de France, 1991 , # 6 p. 904 - 910
反应条件
Porcine Pancreas Lipase in hexane T=20°C; 3 h; Enzymatic reaction; Title compound not separated from byproducts;
参考文献
Zada, Anat; Harel, Miriam
Tetrahedron Asymmetry, 2004 , vol. 15, # 15 p. 2339 - 2343
