拉凡醇; 5-甲基-2-(1-甲基乙烯基)-4-己烯-1-醇合成路线 （共 65 条）
反应条件
pyridine in diethyl ether T=0 - 20°C;
参考文献
Kuraray Co., Ltd.
Patent: EP2119693 A1, 2009 ;
Location in patent: Page/Page column 5 ;
反应条件
pyridine in diethyl ether
cooling;
参考文献
Zada, Anat; Harel, Miriam
Tetrahedron Asymmetry, 2004 , vol. 15, # 15 p. 2339 - 2343
反应条件
1: With lipase in diethyl ether
T=20°C; 48 h; Resolution of racemateEnzymatic reaction;
2: With sodium carbonate in diethyl ether; water
0.5 h;
3: With sodium hydroxide in water
5 h;
参考文献
KEELE UNIVERSITY; KIRK, William Daniel John; HAMILTON, James Gordon Campbell
Patent: WO2014/68303 A1, 2014 ;
Location in patent: Page/Page column 35-36 ;
反应条件
Porcine Pancreas Lipase in hexane
T=20°C; 3 h; Enzymatic reaction; Title compound not separated from byproducts;
参考文献
Zada, Anat; Harel, Miriam
Tetrahedron Asymmetry, 2004 , vol. 15, # 15 p. 2339 - 2343
反应条件
hog pancreas lipase in diethyl ether
T=20°C; 48 h;
参考文献
Zada, Anat; Dunkelblum, Ezra
Tetrahedron Asymmetry, 2006 , vol. 17, # 2 p. 230 - 233
