苯甲酸,1,1'-(二丁基锡烷亚基)酯合成路线 （共 9 条）
反应条件
in toluene molar ratio Cp2V/Sn-compound 1/2, sealed ampoule, 20°C, 24 h;
参考文献
Latyaeva, V. N.; Lineva, A. N.; Zimina, S. V.; Gordetsov, A. S.; Lergunov, Yu. I.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 921 - 926
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 1101 - 1106
反应条件
in toluene molar ratio Cp2V/Sn-compound 1/1, sealed ampoule, 20°C, 24 h; ppt. of V-complex washing (toluene), drying; elem. anal.; solvent removal, fractioning;
参考文献
Latyaeva, V. N.; Lineva, A. N.; Zimina, S. V.; Gordetsov, A. S.; Lergunov, Yu. I.
Journal of General Chemistry USSR (English Translation), 1981 , vol. 51, p. 921 - 926
Zhurnal Obshchei Khimii, 1981 , vol. 51, p. 1101 - 1106
反应条件
in toluene molar ratio Cp2V/Sn-compound 1/2, sealed ampoule, 20°C, 24 h;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 51, p. 921 - 926
Zhurnal Obshchei Khimii, , vol. 51, p. 1101 - 1106
反应条件
in toluene molar ratio Cp2V/Sn-compound 1/1, sealed ampoule, 20°C, 24 h; ppt. of V-complex washing (toluene), drying; elem. anal.; solvent removal, fractioning;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 51, p. 921 - 926
Zhurnal Obshchei Khimii, , vol. 51, p. 1101 - 1106
反应条件
in toluene molar ratio Cp2V/Sn-compound 1/2, sealed ampoule, 20°C, 24 h;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 51, p. 921 - 926
Zhurnal Obshchei Khimii, , vol. 51, p. 1101 - 1106
反应条件
in toluene molar ratio Cp2V/Sn-compound 1/1, sealed ampoule, 20°C, 24 h; ppt. of V-complex washing (toluene), drying; elem. anal.; solvent removal, fractioning;
参考文献
Journal of General Chemistry USSR (English Translation), , vol. 51, p. 921 - 926
Zhurnal Obshchei Khimii, , vol. 51, p. 1101 - 1106
参考文献
Sawyer; Kuivila
Journal of the American Chemical Society, 1960 , vol. 82, p. 5958
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Sawyer; Kuivila
Journal of Organic Chemistry, 1962 , vol. 27, p. 837
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Sawyer, A. K.; Kuivila, H. G.
Journal of Organic Chemistry, 1962 , vol. 27, p. 610 - 614
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.2.1.5.4, page 106 - 110
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Metal & Thermit Corp.
Patent: US3083217 , 1963 ;
C. A., 1963 , vol. 59, p. 7559
反应条件
in neat (no solvent)
Kinetics; byproducts: C2H4; thermal decompn. (110°C, 2 h);
参考文献
Jousseaume, Bernard; Gouron, Veronique; Maillard, Bernard; Pereyre, Michel; Frances, Jean-Marc
Organometallics, 1990 , vol. 9, p. 1330 - 1331
反应条件
in benzene
byproducts: H2; reaction at 60°C;;
参考文献
Vyazankin, N. S.; Bychkov, V. T.
Zhurnal Obshchei Khimii, 1965 , vol. 35, p. 685 - 687
Zhurnal Obshchei Khimii, 1965 , vol. 35, p. 684 - 687
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Gmelin Handbook: Sn: Org.Verb.4, 1.2.2.1.5.4, page 106 - 110
