1-乙基-1H-吲哚-3-甲醛合成路线 （共 14 条）
反应条件
potassium carbonate in acetone 5 h; Heating;
参考文献
Le Borgne, Marc; Marchand, Pascal; Duflos, Muriel; Delevoye-Seiller, Benedicte; Piessard-Robert, Sylvie; Le Baut, Guillaume; Hartmann, Rolf W.; Palzer
Archiv der Pharmazie, 1997 , vol. 330, # 5 p. 141 - 145
反应条件
2,2'-azo-bisisobutyronitrile; tri-n-butyl-tin hydride in benzene T=100°C; Carbonylation; cyclization; P=60800 Torr; 3 h;
参考文献
Tetrahedron Letters, , vol. 40, # 40 p. 7153 - 7157
反应条件
potassium carbonate; copper dichloride in acetonitrile 3 h; Reflux;
参考文献
Zhang, Lei; Peng, Chen; Zhao, Dan; Wang, Yue; Fu, Hai-Jian; Shen, Qi; Li, Jian-Xin
Chemical Communications, 2012 , vol. 48, # 47 p. 5928 - 5930
反应条件
potassium carbonate in acetone Alkylation;
参考文献
Le Borgne; Marchand; Duflos; Robert-Piessard; Le Baut; Ahmadi; Hartmann; Palzer
Pharmaceutical Sciences, 1997 , vol. 3, # 5-6 p. 279 - 281
反应条件
1,1,1,2,2,2-hexabutyl-distannane in benzene T=80°C; Irradiation;
参考文献
Tetrahedron Letters, , vol. 41, # 52 p. 10181 - 10184
反应条件
sodium hydride in N,N-dimethyl-formamide 0.5 h; Ambient temperature;
参考文献
Gatti; Cavrini; Roveri; Luglio
Archiv der Pharmazie, 1985 , vol. 318, # 2 p. 157 - 160
反应条件
1: sodium hydroxide / tetrahydrofuran / Reflux 2: trichlorophosphate / 0 - 20 °C View Scheme
参考文献
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, , vol. 86, p. 640 - 644
反应条件
1: 98 percent / NaI / acetonitrile / 24 h / Heating 2: 32 percent / n-Bu3SnH; AIBN / benzene / 3 h / 100 °C / 60800 Torr View Scheme
参考文献
Tetrahedron Letters, , vol. 40, # 40 p. 7153 - 7157
反应条件
trichlorophosphate T=0 - 20°C; Vilsmeier-Haack reaction;
参考文献
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, , vol. 86, p. 640 - 644
反应条件
N-benzyl-N,N,N-triethylammonium chloride; potassium carbonate T=20°C;
参考文献
Heteroatom Chemistry, , vol. 23, # 1 p. 41 - 48
