Alpha,Alpha-二甲基苄胺合成路线 (共 46 条)
反应条件
lithium aluminium tetrahydride in diethyl ether T=0 - 20°C; 18 h;
参考文献
Metallinos, Costa; Nerdinger, Sven; Snieckus, Victor
Organic Letters, 1999 , vol. 1, # 8 p. 1183 - 1186
反应条件
potassium cyanide; sulfuric acid in anhydrous butyl ether T=60 - 80°C;
参考文献
Bulletin de la Societe Chimique de France, , p. 2319 - 2324
反应条件
cerium(III) chloride
参考文献
Engel; Pan; Ying; Alemany
Journal of the American Chemical Society, 2001 , vol. 123, # 16 p. 3706 - 3715
参考文献
Kamer, Paul C. J.; Nolte, Roeland J. M.; Drenth, Wiendelt
Journal of the American Chemical Society, 1988 , vol. 110, # 20 p. 6818 - 6825
反应条件
1: NaN3, Cl3CCOOH / CHCl3 / 2 h / Heating 2: 61.5 percent / LiAlH4 / diethyl ether / 4 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 102, # 1 p. 259 - 267
反应条件
potassium hydroxide; nickel in ethanol T=20°C; Reduction; pH=13; Electrolysis;
参考文献
Canadian Journal of Chemistry, , vol. 77, # 5-6 p. 687 - 694
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 37, p. 83
Journal of the Chemical Society, , p. 262
反应条件
hydrogenchloride in water 70-80 deg C, 0.5 h; reflux, 0.5 h;
参考文献
Sato, Kazuo; Honma, Toyokuni; Sugai, Soji
Agricultural and Biological Chemistry, 1985 , vol. 49, # 12 p. 3563 - 3568
反应条件
1: in tetrahydrofuran; diethyl ether T=100°C; Double Grignard addition; 0.166667 h; Microwave irradiation; 2: With titanium(IV) isopropylate in tetrahydrofuran; diethyl ether T=50°C; Double Grignard addition; 1 h; Microwave irradiation;
参考文献
Tetrahedron Letters, , vol. 50, # 50 p. 7070 - 7073
反应条件
potassium hydroxide in ethylene glycol
参考文献
Chemische Berichte, , vol. 106, p. 1083 - 1098