(2E,4E)-5-苯基-戊-2,4-二烯-1-醇合成路线 （共 6 条）
反应条件
phosphorus tribromide in diethyl ether T=0°C; 1.5 h;
参考文献
Kim, Dwight D.; Lee, Suk Joong; Beak, Peter
Journal of Organic Chemistry, 2005 , vol. 70, # 14 p. 5376 - 5386
反应条件
(tributylphosphoranylidene)acetonitrile in benzene Ambient temperature;
参考文献
Feldman, Ken S.; Mareska, David A.
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5650 - 5660
反应条件
Aufbewahren an der Luft;
参考文献
Journal of the American Chemical Society, , vol. 69, p. 2926
反应条件
ethanol; nickel Hydrogenation;
参考文献
Nasarow; Fischer
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1948 , p. 436,441
Chem.Abstr., 1949 , p. 2576
反应条件
1: 81 percent / NEt3 / diethyl ether / 3 h / Ambient temperature 2: NEt3 / PdCl2(PPh3)2 / benzene / 3 h / 140 °C / 38000 Torr / effects of catalysts; also for other substituted 2,4-pentadienyl acetates or o-(bromomethyl)(1-alkenyl)benzenes View Scheme
参考文献
Ishii, Youichi; Gao, Chao; Xu, Wen-Xiang; Iwasaki, Masakazu; Hidai, Masanobu
Journal of Organic Chemistry, 1993 , vol. 58, # 24 p. 6818 - 6825
反应条件
1: N-bromosuccinmide; dimethylsulfide / dichloromethane / 0.17 h / |Inert atmosphere
2: cupric bromide-dimethyl sulfide; (R)-(S)-PPF-PCy2 / dichloromethane / 1 h / |Inert atmosphere
View Scheme
参考文献
Huang, Yange; Fananas-Mastral, Martin; Minnaard, Adriaan J.; Feringa, Ben L.
Chemical Communications, 2013 , vol. 49, # 32 p. 3309 - 3311
