反应条件
1: 77 percent / dimethyl sulphide, N-chlorosuccinimide / toluene / 2 h / -25 °C 2: 97 percent / K2CO3 / toluene; diethyl ether / 0 deg C, 1 h and then RT, 3 h 3: 1) 0 deg C, 4 h, and RT, 15 h, then reflux, 48h, methanol, 2) acetic acid, water, reflux, 8 h View Scheme
参考文献
Blowers, John W.; Saxton, J. Edwin; Swanson, Alistair G.
Tetrahedron, 1986 , vol. 42, # 21 p. 6071 - 6095
