(9ci)-2-戊基-1H-苯并咪唑合成路线 （共 13 条）
反应条件
lead dioxide
T=20°C; 0.833333 h; Neat (no solvent);
参考文献
Patil, Vishvanath D.; Patil, Jaymala; Rege, Priyanka; Dere, Ganesh
Synthetic Communications, 2011 , vol. 41, # 1 p. 58 - 62
反应条件
5 palladium on charcoal in water; toluene
T=110°C; 20 h; Inert atmosphere;
参考文献
Tran, Ngoc Thang; Cho, Chan Sik
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 12 p. 4188 - 4190
反应条件
5 palladium on charcoal in water; toluene
T=110°C; 40 h; Inert atmosphere;
参考文献
Tran, Ngoc Thang; Cho, Chan Sik
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 12 p. 4188 - 4190
反应条件
1: [3H]-Caproic acid in dichloromethane
T=0°C; 0.25 h;
2: 1,2-diamino-benzene With pyridine in dichloromethane
T=20°C; 6 h; Further stages.;
参考文献
Kaul, Savita; Kumar, Ajay; Sain, Bir; Bhatnagar
Synthetic Communications, 2007 , vol. 37, # 15 p. 2457 - 2460
反应条件
5 palladium on charcoal in water; toluene
T=110°C; 40 h; Inert atmosphere;
参考文献
Tran, Ngoc Thang; Cho, Chan Sik
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 12 p. 4188 - 4190
反应条件
[Py(NP(iPr)2)(NHP(iPr)2)Ir(cod)]; potassium tert-butylate in diethylene glycol dimethyl ether
T=110°C; 24 h; Inert atmosphere;
参考文献
Hille, Toni; Irrgang, Torsten; Kempe, Rhett
Chemistry - A European Journal, 2014 , vol. 20, # 19 p. 5569 - 5572
反应条件
1: 1,2-diamino-benzene With diethylaluminium chloride in toluene
T=0 - 20°C;
2: hydroxymethyl JandaJelTM resin-bound n-pentyl ester in toluene
24 h; Heating; Further stages.;
参考文献
Matsushita, Hana; Lee, Sang-Hyeup; Joung, Meyoungju; Clapham, Bruce; Janda, Kim D.
Tetrahedron Letters, 2004 , vol. 45, # 2 p. 313 - 316
反应条件
ytterbium trichloride in ethanol
T=20°C; 24 h;
参考文献
Cai, Lijian; Ji, Xiaofeng; Yao, Zhigang; Xu, Fan; Shen, Qi
Chinese Journal of Chemistry, 2011 , vol. 29, # 9 p. 1880 - 1886
反应条件
1: With copper(l) iodide; 4-toluenesulfonyl azide; triethylamine in acetonitrile
T=20°C; 6 h; Inert atmosphere;
2: With sulfuric acid in acetonitrile
4 h; Reflux;
参考文献
She, Jin; Jiang, Zheng; Wang, Yanguang
Synlett, 2009 , # 12 p. 2023 - 2027
反应条件
in ethylene glycol
0.025 h; microwave irradiation;
参考文献
Jing, Xiaobi; Zhu, Qihua; Xu, Feng; Ren, Xinfeng; Li, Dong; Yan, Chaoguo
Synthetic Communications, 2006 , vol. 36, # 18 p. 2597 - 2601
