5-苯基-1,3,4-氧噻唑-2-酮合成路线 （共 21 条）
参考文献
Koval', I. V.; Tarasenko, A. I.; Panchenko, I. S.; Molchanova, N. R.
Journal of Organic Chemistry USSR (English Translation), 1986 , p. 1538 - 1541
Zhurnal Organicheskoi Khimii, 1986 , vol. 22, # 8 p. 1712 - 1715
反应条件
in 1,1,2,2-tetrachloroethylene
Heating;
参考文献
Senning,A.; Kelly,P.
Acta Chemica Scandinavica (1947-1973), 1967 , vol. 21, p. 1871 - 1878
反应条件
in ethyl acetate
T=170°C; 0.5 h; Microwave irradiation;
参考文献
Fordyce, Euan A.F.; Morrison, Angus J.; Sharp, Robert D.; Paton, R. Michael
Tetrahedron, 2010 , vol. 66, # 35 p. 7192 - 7197
反应条件
in 1,3,5-trimethyl-benzene
Heating;
参考文献
McKie, Marion C.; Paton, R. Michael
Journal of Chemical Research, Miniprint, 1987 , # 8 p. 2051 - 2066
反应条件
in 1,2-dichloro-benzene
参考文献
Morrison, Angus J.; Paton, R. Michael; Sharp, Robert D.
Synthetic Communications, 2005 , vol. 35, # 6 p. 807 - 813
反应条件
1: chlorobenzene
2: aq. NaOH
3: 1,2-dichloro-benzene / Heating
4: (i) SOCl2, (ii) /BRN= 1718733/
View Scheme
参考文献
Franz,J.E.; Black,L.L.
Tetrahedron Letters, 1970 , p. 1381 - 1384
反应条件
1: 67 percent / chlorobenzene / 22 h / 130 °C
2: 45 percent / LiAlH4 / diethyl ether / 0.75 h / Heating
3: 75 percent / Et3N / CH2Cl2 / 26 h / Heating
View Scheme
参考文献
Anderson; Jones
Journal of Medicinal Chemistry, 1984 , vol. 27, # 12 p. 1559 - 1565
反应条件
in para-xylene
T=160°C; 0.166667 h; Microwave irradiation;
参考文献
Fordyce, Euan A.F.; Morrison, Angus J.; Sharp, Robert D.; Paton, R. Michael
Tetrahedron, 2010 , vol. 66, # 35 p. 7192 - 7197
反应条件
1: chlorobenzene
2: aq. EtOH
View Scheme
参考文献
Franz,J.E. et al.
Journal of Organic Chemistry, 1976 , vol. 41, p. 620 - 626
反应条件
trimeric thionitrosyl chloride in chlorobenzene
20 h; Heating;
参考文献
Bridson, John N.; Copp, Steven B.; Schriver, Melbourne J.; Zhu, Shuguang; Zaworotko, Michael J.
Canadian Journal of Chemistry, 1994 , vol. 72, # 9 p. 1143 - 1153
