1-乙基-1,3-二氢-5-甲基-2H-苯并咪唑-2-酮合成路线 （共 5 条）
反应条件
1: palladium/charcoal; ethanol / Hydrogenation
2: aqueous HCl
View Scheme
参考文献
Clark; Pessolano
Journal of the American Chemical Society, 1958 , vol. 80, p. 1662
反应条件
1: H2SO4; acetic acid
2: palladium/charcoal; ethanol / Hydrogenation
3: aqueous HCl
View Scheme
参考文献
Clark; Pessolano
Journal of the American Chemical Society, 1958 , vol. 80, p. 1662
参考文献
Clark; Pessolano
Journal of the American Chemical Society, 1958 , vol. 80, p. 1662
反应条件
1: 53 percent / KOH / xylene; ethanol; H2O / 5 h / 150 °C
2: 1.) K2CO3, BuN(1+)*HSO4(1-), 2.) aq. HCl / 1.) CH3CN, reflux, 2.) reflux
View Scheme
参考文献
Gomez-Parra, Vicente; Jimenez, Mercedes; Sanchez, Felix; Torres, Tomas
Liebigs Annalen der Chemie, 1989 , p. 539 - 544
反应条件
hydrogenchloride; tetra(n-butyl)ammonium hydrogensulfate; potassium carbonate
1.) CH3CN, reflux, 2.) reflux; Multistep reaction;
参考文献
Gomez-Parra, Vicente; Jimenez, Mercedes; Sanchez, Felix; Torres, Tomas
Liebigs Annalen der Chemie, 1989 , p. 539 - 544
