3-(溴甲基)-1-甲苯磺酰-1H-吲哚合成路线 （共 6 条）
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane
0.333333 h; Heating / reflux;
参考文献
Le Borgne, Marc; Na, Young Min; Pagniez, Fabrice; Le Baut, Guillaume; Le Pape, Patrice; Abdala, Hiam
Patent: US2004/67998 A1, 2004 ;
Location in patent: Page/Page column 27 ;
反应条件
phosphorus tribromide in diethyl ether
T=0°C; Bromination; 3 h;
参考文献
Marchand; Le Borgne; Duflos; Robert-Piessard; Le Baut; Ahmadi; Hartmann; Palzer
Pharmacy and Pharmacology Communications, 1998 , vol. 4, # 4 p. 211 - 218
反应条件
1: NaBH4
2: 1.30 g / bromine; PPh3 / CCl4
View Scheme
参考文献
Bassoli, Angela; Borgonovo, Gigliola; Busnelli, Gilberto; Morini, Gabriella; Merlini, Lucio
European Journal of Organic Chemistry, 2005 , # 12 p. 2518 - 2525
反应条件
1: NaBH4
2: 1.30 g / bromine; PPh3 / CCl4
View Scheme
参考文献
Bassoli, Angela; Borgonovo, Gigliola; Busnelli, Gilberto; Morini, Gabriella; Merlini, Lucio
European Journal of Organic Chemistry, 2005 , # 12 p. 2518 - 2525
反应条件
1: NaBH4
2: 1.30 g / bromine; PPh3 / CCl4
View Scheme
参考文献
Bassoli, Angela; Borgonovo, Gigliola; Busnelli, Gilberto; Morini, Gabriella; Merlini, Lucio
European Journal of Organic Chemistry, 2005 , # 12 p. 2518 - 2525
反应条件
potassium carbonate in acetonitrile
T=60°C; 9 h;
参考文献
Yabe, Osamu; Mizufune, Hideya; Ikemoto, Tomomi
Synlett, 2009 , # 8 p. 1291 - 1294
