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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
蛋氨酸-脑啡呔
合成路线
（共 62 条）
1188307-69-8
→
反应条件
41833-13-0
4-羟基-3-硝基苄醇
+
58569-55-4
蛋氨酸-脑啡呔
反应条件
Escherichia coli EC 32123 β-galactosidase in dimethyl sulfoxide T=37°C; pH=7; 0.166667 h; aq. phosphate bufferEnzymatic reaction;
参考文献
Angewandte Chemie, International Edition, , vol. 48, # 35 p. 6443 - 6447
Angewandte Chemie, , vol. 121, # 35 p. 6565 - 6569
59481-77-5
BOC-MET-ENKEPHALIN
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
hydrogenchloride; acetic acid 1 h;
参考文献
Masiukif.wicx, Elzbieta; Rzeszotarska, Barbara
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 11 p. 1672 - 1675
60283-51-4
(蛋氨酰(O)5)-脑啡肽
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
NH4I; dimethylsulfide in trifluoroacetic acid T=0°C;
参考文献
Tetrahedron, , vol. 54, # 50 p. 15273 - 15286
70035-46-0
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
1: 90 percent / HOBt*H2O, NEt3, DCC / dimethylformamide / a) -5 deg C to 0 deg C, 1 h, b) 20 deg C, 24 h 2: 86 percent / 0.5 M NaOH / acetone / 1.5 h 3: 90 percent / 1.3 M HCl/AcOH / 1 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 46, # 11 p. 1672 - 1675
129398-68-1
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
trifluorormethanesulfonic acid; methyl-phenyl-thioether; ethane-1,2-dithiol; 3-methyl-phenol; trifluoroacetic acid T=0°C; 1.5 h;
参考文献
Futaki, Shiroh; Yagami, Takeshi; Taike, Takashi; Akita, Tadashi; Kitagawa, Kouki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 653 - 658
1161-13-3
N-苄氧羰基-L-苯丙氨酸
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
1: 45 percent / DCC / acetonitrile / -10 °C 2: palladium / ethanol; cyclohexene / 0.5 h / Heating 3: 59 percent / DCC, 1-hydroxybenzotriazole / acetonitrile; dimethylformamide / -10 °C 4: palladium / ethanol / 0.5 h / Heating 5: 46 percent / dimethylformamide / 4 °C 6: 74 percent / thioanisole, trifluoroacetic acid / 1 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 581 - 585
4976-72-1
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
1: 45 percent / DCC / acetonitrile / -10 °C 2: palladium / ethanol; cyclohexene / 0.5 h / Heating 3: 59 percent / DCC, 1-hydroxybenzotriazole / acetonitrile; dimethylformamide / -10 °C 4: palladium / ethanol / 0.5 h / Heating 5: 46 percent / dimethylformamide / 4 °C 6: 74 percent / thioanisole, trifluoroacetic acid / 1 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 581 - 585
16874-01-4
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
1: palladium black / ethanol; cyclohexene / 3 h / Heating 2: 45 percent / DCC / acetonitrile / -10 °C 3: palladium / ethanol; cyclohexene / 0.5 h / Heating 4: 59 percent / DCC, 1-hydroxybenzotriazole / acetonitrile; dimethylformamide / -10 °C 5: palladium / ethanol / 0.5 h / Heating 6: 46 percent / dimethylformamide / 4 °C 7: 74 percent / thioanisole, trifluoroacetic acid / 1 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 581 - 585
82362-13-8
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
1: 59 percent / DCC, 1-hydroxybenzotriazole / acetonitrile; dimethylformamide / -10 °C 2: palladium / ethanol / 0.5 h / Heating 3: 46 percent / dimethylformamide / 4 °C 4: 74 percent / thioanisole, trifluoroacetic acid / 1 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 581 - 585
82362-12-7
→
反应条件
58569-55-4
蛋氨酸-脑啡呔
反应条件
1: palladium / ethanol; cyclohexene / 0.5 h / Heating 2: 59 percent / DCC, 1-hydroxybenzotriazole / acetonitrile; dimethylformamide / -10 °C 3: palladium / ethanol / 0.5 h / Heating 4: 46 percent / dimethylformamide / 4 °C 5: 74 percent / thioanisole, trifluoroacetic acid / 1 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 30, # 2 p. 581 - 585
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