1: With 2,2,6,6-tetramethylpiperidinyl-lithium in tetrahydrofuran T=0°C; 2 h; 2: With 1,2,2-trichloro-1,1,2-trichloro-ethane in tetrahydrofuran T=0 - 65°C; 2.5 h; 3: With hydrogenchloride T=20°C;
参考文献
Nguyen, Thi-Huu; Chau, Nguyet Trang Thanh; Castanet, Anne-Sophie; Nguyen, Kim Phi Phung; Mortier, Jacques
Journal of Organic Chemistry, 2007 , vol. 72, # 9 p. 3419 - 3429
1: With n-butyllithium; potassium tert-butylate in tetrahydrofuran T=-78 - -50°C; 2 h; 2: With 1,1-dibromo-tetrachloro-ethane in tetrahydrofuran T=-50°C; 0.5 h; 3: With hydrogenchloride T=20°C;
参考文献
Nguyen, Thi-Huu; Chau, Nguyet Trang Thanh; Castanet, Anne-Sophie; Nguyen, Kim Phi Phung; Mortier, Jacques
Organic Letters, 2005 , vol. 7, # 12 p. 2445 - 2448
