反应条件
1: O,N-dimethyl-hydroxylamine hydrochloride; triethylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 18 h / 20 °C
2: tetrahydrofuran / 4 h / 0 - 20 °C
3: [(η5-C5Me5)2Rh2(μ-Cl)2Cl2]; oxygen; caesium carbonate / methanol / 12 h / 65 °C / |Sealed tube
View Scheme
参考文献
Chan, Louis K. M.; Poole, Darren L.; Shen, Di; Healy, Mark P.; Donohoe, Timothy J.
Angewandte Chemie - International Edition, 2014 , vol. 53, # 3 p. 761 - 765
Angew. Chem., 2014 , vol. 126, # 3 p. 908