sodium hydroxide; palladium diacetate in water T=140°C; Hiyama reaction; 3 h;
参考文献
Gordillo, Alvaro; Ortuno, Manuel A.; Lopez-Mardomingo, Carmen; Lledos, Agusti; Ujaque, Gregori; De Jesus, Ernesto
Journal of the American Chemical Society, 2013 , vol. 135, # 37 p. 13749 - 13763
1: With n-butyllithium in tetrahydrofuran; hexane; toluene T=-70°C; 1.5 h; 2: With tri-isopropoxy-borane in tetrahydrofuran; hexane; toluene T=-70 - -20°C; Further stages.;
参考文献
Li, Wenjie; Nelson, Dorian P.; Jensen, Mark S.; Hoerrner, R. Scott; Cai, Dongwei; Larsen, Robert D.; Reider, Paul J.
Journal of Organic Chemistry, 2002 , vol. 67, # 15 p. 5394 - 5397
1: vinyl-triethoxy-silane With sodium hydroxide in water T=20°C; 0.0833333 h; Sealed tube; 2: 4-bromophenylacetic acid With palladium diacetate in water T=120 - 140°C; Sealed tube;
参考文献
Gordillo, Alvaro; Ortuno, Manuel A.; Lopez-Mardomingo, Carmen; Lledos, Agusti; Ujaque, Gregori; De Jesus, Ernesto
Journal of the American Chemical Society, 2013 , vol. 135, # 37 p. 13749 - 13763