反应条件
1: 1-bromo-4-nitro-benzene With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; N-ethyl-N,N-diisopropylamine in acetonitrile Sonogashira cross-coupling; 0.333333 h; Inert atmosphere; 2: anhydrous 1-octyne in acetonitrile T=50°C; Sonogashira cross-coupling; Inert atmosphere;
参考文献
Sorensen, Jakob Kryger; Fock, Jeppe; Pedersen, Anders Holmen; Petersen, Asger B.; Jennum, Karsten; Bechgaard, Klaus; Kilsa, Kristine; Geskin, Victor; Cornil, Jerome; Bjornholm, Thomas; Nielsen, Mogens Brondsted
Journal of Organic Chemistry, 2011 , vol. 76, # 1 p. 245 - 263