反应条件
in tetrahydrofuran Nitrosobenzene soln. in THF under N2 is stirred at 25°C until it is light blue in color, to this soln. is added carbene complex in THF, the soln. is heated under reflux.; cooling of resulting olive green soln. to 25°C, solvent removal, residue is dissolved in CH2Cl2, filtn., solvent removal from orange filtrate, residue is dissolved in a 19:1 hexane:ethyl acetate soln., purifn. by chromy., three fractions;
参考文献
Herndon, James W.; McMullen, Leonard A.
Journal of Organometallic Chemistry, 1989 , vol. 368, p. 83 - 102
