1: 1.) 1,2-dibromoethane, magnesium / 1.) benzene, THF, 2.) -45 deg C -> room temperature, 15 min
2: air / chromatography on SiO2
3: 170 mg / CHCl3 / 168 h / Ambient temperature; in the dark
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
1: 1.) 1,2-dibromoethane, magnesium / 1.) benzene, THF, 2.) -45 deg C -> room temperature, 15 min
2: air / chromatography on SiO2
3: 60 mg / CHCl3 / 168 h / Ambient temperature; in the dark
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764
1: 1.) 1,2-dibromoethane, magnesium / 1.) benzene, THF, 2.) -45 deg C -> room temperature, 15 min
2: air / chromatography on SiO2
3: 85 percent / benzene / 336 h / Ambient temperature; in the dark
View Scheme
参考文献
Forrester, Alexander R.; Fullerton, Joseph D.; McConnachie, Gordon
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1759 - 1764