2,4-二硝基苯乙酸甲酯合成路线 （共 16 条）
反应条件
in methanol; toluene T=20°C; 3 h;
参考文献
Schering AG
Patent: US2004/39019 A1, 2004 ;
Location in patent: Page/Page column 5-6 ;
US 20040039019 A1
参考文献
Chemische Berichte, , vol. 42, p. 1317
Chemische Berichte, , vol. 21, p. 1307
反应条件
sodium hydride in N,N-dimethyl-formamide T=-10°C; 4 h;
参考文献
Maruoka, Hiroshi; Tomioka, Yukihiko
Journal of Heterocyclic Chemistry, 2003 , vol. 40, # 6 p. 1051 - 1057
反应条件
potassium tert-butylate in ethylene glycol dimethyl ether T=-20 - 0°C;
参考文献
Synthesis, , # 3 p. 242 - 243
反应条件
potassium tert-butylate in ethylene glycol dimethyl ether T=-20 - 0°C;
参考文献
Synthesis, , # 3 p. 242 - 243
反应条件
1: sulfuric acid; potassium nitrate / 60 °C 2: sulfuric acid View Scheme
参考文献
Farmaco (1946-1952), , vol. 3, p. 509,523
反应条件
1: With hydrogen; palladium 10 on activated carbon in ethylene glycol dimethyl ether; ethanol P=2585.81 Torr; 2: With hydrogenchloride in water 0.333333 h; Heating / reflux; 3: With sodium hydroxide in water
参考文献
Carruthers, Nicholas I.; Chai, Wenying; Dax, Scott L.; Jablonowski, Jill A.; Li, Xiaobing; Lovenberg, Timothy W.; Murray, William V.; Rudolph, Dale A.; Seierstad, Mark; Youngman, Mark A.
Patent: US2005/70534 A1, 2005 ;
Location in patent: Page/Page column 13 ;
US 20050070534 A1
反应条件
ethanol anschliessend Behandeln mit aethanol. KOH und Erwaermen der danach erhaltenen Loesung mit wss. Na2CO3;
参考文献
Sabnis; Shirsat
Journal of Scientific and Industrial Research, 1958 , vol. 17 B, p. 451,454
反应条件
2: triethylamine; toluene 3: platinum; ethanol / Hydrogenation View Scheme
参考文献
Journal of the American Chemical Society, , vol. 74, p. 2226,2235
反应条件
2: triethylamine; toluene View Scheme
参考文献
Clinton; Laskowski
Journal of the American Chemical Society, 1952 , vol. 74, p. 2226,2235
