2,6-双(氯甲基)-4-甲酚合成路线 （共 17 条）
参考文献
Ziegler; Luedde
Monatshefte fuer Chemie, 1948 , vol. 79, p. 316,319
参考文献
Ziegler
Monatshefte fuer Chemie, 1948 , vol. 78, p. 334,340
反应条件
triethylamine in tetrahydrofuran
96 h; Ambient temperature;
参考文献
Borovik, A. S.; Papaefthymiou, Vasilios; Taylor, Lucille F.; Anderson, Oren P.; Que, Lawrence
Journal of the American Chemical Society, 1989 , vol. 111, # 16 p. 6183 - 6195
反应条件
N-ethyl-N,N-diisopropylamine in methanol; dichloromethane
T=20°C; 48 h; Cooling;
参考文献
Zee, Yoke Leng Michelle; Gahan, Lawrence R.; Schenk, Gerhard
Australian Journal of Chemistry, 2011 , vol. 64, # 3 p. 258 - 264
反应条件
1: 78 percent / NaOMe / 12 h
2: PhI(OAc)2 / CH2Cl2 / 2.5 h / 20 °C
3: 52 percent / Dess Martin periodinane / CH2Cl2 / 1 h / 20 °C
View Scheme
参考文献
Liu, Qin; Rovis, Tomislav
Journal of the American Chemical Society, 2006 , vol. 128, # 8 p. 2552 - 2553
反应条件
1: 78 percent / NaOMe / 12 h
2: PhI(OAc)2 / CH2Cl2 / 2.5 h / 20 °C
View Scheme
参考文献
Liu, Qin; Rovis, Tomislav
Journal of the American Chemical Society, 2006 , vol. 128, # 8 p. 2552 - 2553
反应条件
in xylene
Arbuzov reaction; Heating;
参考文献
Matveeva; Matrosov; Starikova; Bodrin; Matveev; Petrovskii; Nifant'ev
Russian Chemical Bulletin, 2005 , vol. 54, # 11 p. 2519 - 2534
