5-苄氧基-4-甲氧基-2-硝基苯甲醛合成路线 （共 13 条）
反应条件
1: hydrogenchloride; iron / ethanol 2: ethanol / |Reflux 3: peracetic acid; sulfuric acid / ethanol / 10 h / 60 °C View Scheme
参考文献
Jin, Jian-Wen; Zhang, Lin; Meng, Guang-Rong; Zhu, Jian-Hua; Zhang, Qian
Synthetic Communications, 2014 , vol. 44, # 3 p. 346 - 351
反应条件
trifluoroacetic acid T=60°C; Yield given;
参考文献
Dominique, Romyr; Luk, Kin-Chun; Qiao, Qi; Rossman, Pamela Loreen
Patent: US2012/184548 A1, 2012 ;
Location in patent: Page/Page column 44 ;
US 20120184548 A1
反应条件
nitric acid
T=0 - 20°C; 1.5 h;
参考文献
Patteux, Claudine; Foucout, Lenaig; Bohn, Pierre; Dupas, Georges; Leprince, Jerome; Tonon, Marie-Christine; Dehouck, Benedicte; Marsais, Francis; Papamicael, Cyril; Levacher, Vincent
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 5 p. 817 - 825
反应条件
potassium carbonate in N,N-dimethyl-formamide
4 h; Heating;
参考文献
Banwell, Martin G.; Hamel, Ernest; Ireland, Neil K.; Mackay, Maureen F.; Serelis, Algirdas K.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 16 p. 1905 - 1912
反应条件
sodium hydroxide
T=85°C; 1 h;
参考文献
Kobayashi, Shigeru; Okimoto, Kazuto; Imakura, Yasuhiro
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1567 - 1573
反应条件
1.1: potassium carbonate / ethanol / 0.5 h / 20 °C
1.2: 5 h / 100 °C
2.1: nitric acid / dichloromethane / 1 h / 0 - 20 °C
View Scheme
参考文献
Dominique, Romyr; Luk, Kin-Chun; Qiao, Qi; Rossman, Pamela Loreen
Patent: US2012/184548 A1, 2012 ;
US 20120184548 A1
反应条件
1: potassium carbonate / N,N-dimethyl-formamide / 3 h / 90 °C
2: nitric acid / 2 h / 0 - 20 °C
View Scheme
参考文献
Li, Wen-Yan; Xiong, Xu-Qiong; Zhao, Dong-Mei; Shi, Yu-Fang; Yang, Zhi-Heng; Yu, Chao; Fan, Pei-Wei; Cheng, Mao-Sheng; Shen, Jing-Kang
Molecules, 2012 , vol. 17, # 5 p. 5497 - 5507
反应条件
1: 41 percent / phenylmethanol; dimethylsulfoxide / 0.02 h / 150 °C
2: 42 percent / 2 percent NaOH / 1 h / 85 °C
View Scheme
参考文献
Kobayashi, Shigeru; Okimoto, Kazuto; Imakura, Yasuhiro
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1567 - 1573
反应条件
1: 41 percent / phenylmethanol; dimethylsulfoxide / 0.02 h / 150 °C
2: 42 percent / 2 percent NaOH / 1 h / 85 °C
View Scheme
参考文献
Kobayashi, Shigeru; Okimoto, Kazuto; Imakura, Yasuhiro
Chemical & Pharmaceutical Bulletin, 1982 , vol. 30, # 5 p. 1567 - 1573
反应条件
1.1: potassium carbonate / ethanol / 0.5 h / 20 °C
1.2: 5 h / 100 °C
2.1: nitric acid / dichloromethane / 1 h / 0 - 20 °C
View Scheme
参考文献
Dominique, Romyr; Luk, Kin-Chun; Qiao, Qi; Rossman, Pamela Loreen
Patent: US2012/184548 A1, 2012 ;
US 20120184548 A1
