2-氨基-5-甲基苯甲酸乙酯合成路线 （共 6 条）
反应条件
hydrogenchloride in ethanol
参考文献
Masciadri, Raffaello; Thomas, Andrew William; Wichmann, Juergen
Patent: US2003/55042 A1, 2003 ;
反应条件
palladium 10 on activated carbon; hydrogen in ethanol P=760.051 Torr; 168 h; Darkness;
参考文献
Bhuiyan, M. Delower H.; Zhu, Kai-Xian; Jensen, Paul; Try, Andrew C.
European Journal of Organic Chemistry, 2010 , # 24 p. 4662 - 4670
反应条件
hydrogenchloride 2 h; Heating;
参考文献
Kennewell, Peter D.; Scrowston, Richard M.; Shenouda, Ibrahim G.; Tully, W. Roger; Westwood, Robert
Journal of Chemical Research, Miniprint, 1986 , # 7 p. 2001 - 2025
反应条件
dimethylsulfone T=150°C; 1 h;
参考文献
McNamara; Berman; Fry; Werbel
Journal of Medicinal Chemistry, 1990 , vol. 33, # 7 p. 2045 - 2051
反应条件
1: 82 percent / I2; Ag2SO4 / ethanol / 18 h / 20 °C 2: 90 percent / aq. KOH / methanol / 12 h / 50 °C View Scheme
参考文献
Koradin, Christopher; Dohle, Wolfgang; Rodriguez, Alain L.; Schmid, Bertram; Knochel, Paul
Tetrahedron, 2003 , vol. 59, # 9 p. 1571 - 1587
反应条件
1: 86 percent / conc. HCl, CaCO3 / H2O; 1,2-dichloro-ethane / 1 h
2: 93 percent / 100percent N2H4*H2O / ethanol / 3 h / Heating
3: 69 percent / NaNO2, 5M HCl / 0.25 h
View Scheme
参考文献
Kennewell, Peter D.; Scrowston, Richard M.; Shenouda, Ibrahim G.; Tully, W. Roger; Westwood, Robert
Journal of Chemical Research, Miniprint, 1986 , # 7 p. 2001 - 2025
