1: diethyl ether / 1.5 h / -20 °C
2: Jones reagent / acetone / 0.5 h / 0 °C
3: NaH / tetrahydrofuran / room temp., 1 h then 65 deg C 3 h
4: AlH3 / diethyl ether / 1.5 h / -15 - 0 °C
View Scheme
参考文献
Uesato; Kobayashi; Inouye
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 3 p. 927 - 940