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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
3-氯苯甲醛
合成路线
（共 460 条）
587-04-2
3-氯苯甲醛
→
反应条件
33537-99-4
6-氯-1,2,3,4-四氢异喹啉
反应条件
1: LiAlH4 / diethyl ether / Heating 2: H2SO4; AcOH / ethanol / 20 °C 3: HCl / ethanol / Heating View Scheme
参考文献
Bojarski, Andrzej J; Mokrosz, Maria J; Minol, Sijka Charakchieva; Koziol, Aneta; Wesolowska, Anna; Tatarczynska, Ewa; Klodzinska, Aleksandra; Chojnacka-Wojcik, Ewa
Bioorganic and Medicinal Chemistry, 2002 , vol. 10, # 1 p. 87 - 95
587-04-2
3-氯苯甲醛
→
反应条件
34841-39-9
安非他酮
反应条件
1.1: 1,4-diaza-bicyclo[2.2.2]octane / 30 °C / Sonication 2.1: 1H-imidazole; dimethyl sulfoxide / 20 °C / Inert atmosphere 3.1: water; lithium hydroxide hydrate / acetonitrile / 4 h / 50 - 60 °C 4.1: triethylamine / acetone / 0.08 h / 0 °C 5.1: sodium azide / acetone / 2 h / 20 °C 6.1: toluene / 2 h / Reflux; Inert atmosphere 7.1: water / 2 h / Reflux 8.1: sodium tetrahydroborate / methanol / 0.17 h / 0 - 20 °C / Inert atmosphere 9.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C 10.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 30 h / 20 °C 11.1: 2,6-dimethylpyridine; trifluoromethylsulfonic anhydride / dichloromethane / 0.5 h / -78 - -40 °C 11.2: 14 h / -40 - 0 °C View Scheme
参考文献
Amarante, Giovanni W.; Cavallaro, Mayra; Coelho, Fernando
Journal of the Brazilian Chemical Society, 2011 , vol. 22, # 8 p. 1568 - 1584
587-04-2
3-氯苯甲醛
→
反应条件
34841-35-5
3'-氯丙酮苯
反应条件
2: H2CrO4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 41, p. 2368 - 2372
587-04-2
3-氯苯甲醛
+
102-04-5
二苄基甲酮
→
反应条件
103-82-2
苯乙酸
+
14064-67-6
+
14064-43-8
反应条件
boron trifluoride in hexane 5 h; Heating; Yield given. Yields of byproduct given;
参考文献
Kabalka, George W.; Tejedor, David; Li, Nan-Sheng; Malladi, Rama R.; Trotman, Sarah
Tetrahedron, 1998 , vol. 54, # 51 p. 15525 - 15532
→
反应条件
142327-37-5
3-苯硫基苯甲醛
反应条件
1: 3-chloro-benzaldehyde With palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene in N,N-dimethyl-formamide T=20°C; 0.0833333 h; Inert atmosphere; 2: In(SPh)3 With caesium carbonate in N,N-dimethyl-formamide T=100°C; 4 h; Inert atmosphere;
参考文献
Atobe, Shingo; Sonoda, Motohiro; Suzuki, Yuki; Shinohara, Hiroyuki; Yamamoto, Takuya; Ogawa, Akiya
Chemistry Letters, 2011 , vol. 40, # 9 p. 980 - 982
587-04-2
3-氯苯甲醛
+
75-05-8
乙腈
→
反应条件
24654-47-5
反应条件
potassium hydroxide Inert atmosphereReflux; optical yield given as percent de;
参考文献
Ma, Yunhai; Xu, Jiaxi
Synthesis (Germany), 2012 , vol. 44, # 14 art. no. SS-2012-H0334-OP, p. 2225 - 2230
587-04-2
3-氯苯甲醛
→
反应条件
174265-12-4
反应条件
1: pyridine / dichloromethane / 1 h / 20 °C 2: N-bromosuccinmide; Ag(1-)*C2F3O2(1-); palladium diacetate / 1,2-dichloro-ethane / 24 h / 120 °C 3: formaldehyd; toluene-4-sulfonic acid / tetrahydrofuran; water / 0.25 h / 100 °C / Microwave irradiation View Scheme
参考文献
Dubost, Emmanuelle; Fossey, Christine; Cailly, Thomas; Rault, Sylvain; Fabis, Frederic
Journal of Organic Chemistry, 2011 , vol. 76, # 15 p. 6414 - 6420
587-04-2
3-氯苯甲醛
→
反应条件
39191-07-6
反应条件
1: 1 h / 80 °C 2: LiAlH4 / diethyl ether / 2 h / Heating View Scheme
参考文献
Meindl; Von Angerer; Schonenberger; Ruckdeschel
Journal of Medicinal Chemistry, 1984 , vol. 27, # 9 p. 1111 - 1118
587-04-2
3-氯苯甲醛
+
73183-34-3
→
反应条件
380151-86-0
反应条件
tris-(dibenzylideneacetone)dipalladium(0); 2-(2-methoxyphenyl)-1-methyl-3-(diphenylphosphino)-1H-indole; potassium acetate in 1,4-dioxane T=110°C; 24 h; Inert atmosphere;
参考文献
Chow, Wing Kin; Yuen, On Ying; So, Chau Ming; Wong, Wing Tak; Kwong, Fuk Yee
Journal of Organic Chemistry, 2012 , vol. 77, # 7 p. 3543 - 3548
587-04-2
3-氯苯甲醛
+
346713-20-0
→
反应条件
91426-46-9
反应条件
1: in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: With phosphonic acid diethyl ester in tetrahydrofuran Inert atmosphere;
参考文献
Li, Ying; Hu, Yuan-Yuan; Zhang, Song-Lin
Chemical Communications, 2013 , vol. 49, # 90 p. 10635 - 10637
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