双(硫代苯甲酰基)二硫化物合成路线 （共 25 条）
反应条件
iodine in water T=20°C; 0.25 h;
参考文献
Commonwealth Scientific and Industrial Research Organisation
Patent: EP1149075 B1, 2008 ;
Location in patent: Page/Page column 13-14 ;
反应条件
1.1: sodium methylate; sulfur / methanol / 10 h / Inert atmosphere; Reflux 2.1: sodium hydroxide / water 2.2: 1 h View Scheme
参考文献
Journal of Materials Chemistry, , vol. 21, # 34 p. 12682 - 12690
反应条件
1: bromobenzene With magnesium; iodine in tetrahydrofuran 2: carbon disulfide in tetrahydrofuran Grignard reaction; 3: With dimethyl sulfoxide; iodine in ethanol T=20°C; 1 h; Further stages.;
参考文献
Vosloo; De Wet-Roos; Tonge; Sanderson
Macromolecules, 2002 , vol. 35, # 13 p. 4894 - 4902
反应条件
sodium hydroxide; potassium hexacyanoperferrate 0.5 h;
参考文献
Chemical Communications, , # 21 p. 2145 - 2147
反应条件
1: dithiobenzoic acid sodium salt With iodine in water 1 h; 2: V-501 in ethyl acetate 18 h;
参考文献
US2004/138492 A1, ;
Page 3 ;
参考文献
Yu, Lihong; Lo, Kin Cheung; Xi, Jingyu; Phillips, David Lee; Chan, Wai Kin
New Journal of Chemistry, 2013 , vol. 37, # 6 p. 1833 - 1842
反应条件
1.1: iodine; magnesium / tetrahydrofuran / 1 h 1.2: 2 h / 0 °C 2.1: iodine; dimethyl sulfoxide / ethanol / 2 h / 20 °C View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 89, # 3 p. 317 - 325
反应条件
iodine in ethanol T=-5°C; 0.166667 h;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 121 - 128
反应条件
N(Et)4ClO4 in methanol T=80°C; 3 h; electrochemical reaction, 14 mA*cm-2, 2.5 F; Further byproducts given;
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 27, p. 261 - 274
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 22, # 11 p. 2194 - 2198
Zhurnal Organicheskoi Khimii, , vol. 22, # 11 p. 2443 - 2448
