4-溴-4′-甲氧基联苯合成路线 （共 57 条）
反应条件
sodium hydroxide in ethanol; water Heating;
参考文献
Molecular Crystals and Liquid Crystals Science and Technology Section A: Molecular Crystals and Liquid Crystals, , vol. 339, p. 145 - 158
反应条件
1: 3-chloro-benzenecarboperoxoic acid; boron trifluoride diethyl etherate / diethyl ether; dichloromethane 2: trifluoroacetic acid sodium salt / water; dichloromethane 3: 2Na(1+)*H2O*Cl4Pt(2-); acetic acid; tetrabutylammonium trifluoromethanesulphonate / 72 h View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 42 p. 15710 - 15713
反应条件
1: 95 percent / HCl(g) 2: 1.) Wang resin, Huenig's base, 2.) 3percent Pd(PPh3)4, 2M Na2CO3, 3.) Br2, pyridine / 1.) DMF, 40-50 deg C, 2.) DME, reflux, 3.) DMF, 80-90 deg C, 24 h View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 16 p. 2703 - 2706
反应条件
pyridine; tetrakis(triphenylphosphine) palladium(0); bromine; sodium carbonate; N-ethyl-N,N-diisopropylamine; Wang resin 1.) DMF, 40-50 deg C, 2.) DME, reflux, 3.) DMF, 80-90 deg C, 24 h; Yield given. Multistep reaction;
参考文献
Tetrahedron Letters, , vol. 37, # 16 p. 2703 - 2706
参考文献
Journal of the Chemical Society, , p. 1286,1289
参考文献
Journal of the Chemical Society, , p. 1071,1072,1076
Journal of the Chemical Society, , p. 3504
参考文献
Journal of the Chemical Society, , p. 1379,1381
参考文献
Journal of the Chemical Society, , p. 1379,1381
反应条件
2Na(1+)*H2O*Cl4Pt(2-); tetrabutylammonium trifluoromethanesulphonate; acetic acid 72 h; Overall yield = 58percent; Overall yield = 78 mg;
参考文献
Journal of the American Chemical Society, , vol. 135, # 42 p. 15710 - 15713
反应条件
manganese triacetate Heating; Title compound not separated from byproducts.;
参考文献
Journal of the Chemical Society. Perkin Transactions 1, , # 22 p. 3042 - 3045
