N-(2,2-二甲氧基乙基)-4-甲基苯磺酰胺合成路线 （共 4 条）
反应条件
triethylamine in dichloromethane
T=0°C; 0.5 h;
参考文献
Lee, Ge Hyeong; Choi, Eun Bok; Lee, Eun; Pak, Chwang Siek
Journal of Organic Chemistry, 1994 , vol. 59, # 6 p. 1428 - 1443
反应条件
sodium methylate; potassium bromide
T=25°C; anodic oxidation;
参考文献
Shono, Tatsuya; Matsumura, Yoshihiro; Katoh, Susumu; Inoue, Kenji; Matsumoto, Yonetatsu
Tetrahedron Letters, 1986 , vol. 27, # 50 p. 6083 - 6086
反应条件
1.1: NaH / tetrahydrofuran / 0 - 20 °C
1.2: 65 percent / tetrahydrofuran / 36 h / Heating
2.1: 53 percent / aq. HCl / acetone / 48 h
View Scheme
参考文献
Rochette, Elise M.; Lewis, William; Dossetter, Al G.; Stockman, Robert A.
Chemical Communications, 2013 , vol. 49, # 82 p. 9395 - 9397
反应条件
1.1: NaH / dimethylformamide / 0.5 h / 0 °C
1.2: 96 percent / dimethylformamide / 2 h / 20 °C
2.1: 100 percent / aq. HCl / tetrahydrofuran / 3 h / Heating
View Scheme
参考文献
Huang, Long; Yang, Hai-Bin; Zhang, Di-Han; Zhang, Zhen; Tang, Xiang-Ying; Xu, Qin; Shi, Min
Angewandte Chemie - International Edition, 2013 , vol. 52, # 26 p. 6767 - 6771
