4-苯基-3-丁炔-2-醇合成路线 （共 25 条）
反应条件
diethyl ether man gibt Acetaldehyd hinzu und zersetzt das Reaktionsprodukt mit Eis;
参考文献
Bulletin de la Societe Chimique de France, , vol. <3> 33, p. 155
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine 1) hexane, reflux, 3 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 104, # 9 p. 226 - 230
参考文献
Journal of Organic Chemistry, , vol. 57, # 11 p. 3231 - 3236
反应条件
in tetrahydrofuran 16 h; Ambient temperatureoher aldehydes and ketones; also with bis(pentafluorophenyl)ytterbium;
参考文献
Journal of Organometallic Chemistry, , vol. 205, # 1 p. C4 - C6
反应条件
1: N,N-dimethylaminopyridine (DMAP), Et3N / CH2Cl2 / 3 h / Ambient temperature 2: H2, quinoline / Pd (5percent on BaSO4) / 1.5 h 4: 1.) boron trifluoride 2.) aq. sodium hydrogen carbonate / 1.) AcOH, CH2Cl2, 20 deg C, 1.5 h 2.) 15 min 5: Et3N, m-chloroperbenzoic acid / diethyl ether / 20 h / Ambient temperature View Scheme
参考文献
Fleming, Ian; Higgins, Dick; Lawrence, Nicholas J.; Thomas, Andrew P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1992 , # 24 p. 3331 - 3350
