2: 1) BuLi, ZnCl2 / 2) iBu2AlH, Pd(PPh3)2Cl2 / 1) THF, hexane, r.t., 1 h, 2) THF, hexane, r.t., overnight View Scheme

n-butyllithium; zinc(II) chloride; bis-triphenylphosphine-palladium(II) chloride; diisobutylaluminium hydride 1) THF, hexane, r.t., 1 h, 2) THF, hexane, r.t., overnight; Yield given. Multistep reaction;

暂无反应条件数据

Title compound not separated from byproducts;

potassium hydroxide in methanol 3 h; Ambient temperature;