反应条件
1.1: copper(l) iodide; triphenylphosphine; lithium methanolate / N,N-dimethyl-formamide / 18 h / 30 °C / |Schlenk technique; |Inert atmosphere 2.1: sodium periodate / water; tetrahydrofuran / 0.08 h 2.2: 20 °C 3.1: 1,10-phenanthroline; silver carbonate; potassium phosphate; copper(l) iodide; silver fluoride / N,N-dimethyl-formamide / 24 h / 80 °C / |Glovebox; |Inert atmosphere View Scheme
参考文献
Xu, Jun; Xiao, Bin; Xie, Chuan-Qi; Luo, Dong-Fen; Liu, Lei; Fu, Yao
Angewandte Chemie - International Edition, 2012 , vol. 51, # 50 p. 12551 - 12554
Angew. Chem., 2012 , vol. 124, # 50 p. 12719 - 12722,4
