反应条件
1: 1.) tert-butyllithium / 1.) ether, pentane, -78 deg C, 5 h, 2.) a) room temperature, overnight, b) reflux, 14 h 2: 75 percent / m-chloroperbenzoic acid, NaHCO3 / CH2Cl2 / 24 h / Ambient temperature 3: tetraethylammonium fluoride hydrate / acetonitrile View Scheme
参考文献
Chan, T. H.; Chen, L. M.; Wang, D.; Li, L. H.
Canadian Journal of Chemistry, 1993 , vol. 71, # 1 p. 60 - 67