1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 3 h; 2: With boron triethoxide in tetrahydrofuran; hexane T=-78 - 20°C; 3: With hydrogenchloride in tetrahydrofuran; hexane Title compound not separated from byproducts;
参考文献
Fuchibe, Kohei; Akiyama, Takahiko
Journal of the American Chemical Society, 2006 , vol. 128, # 5 p. 1434 - 1435
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2.5 h; 2: With boric acid trimethyl ester in tetrahydrofuran; hexane T=20°C; 8 h; 3: With hydrogenchloride; water in tetrahydrofuran; hexane 1 h;
参考文献
Thiemann, Thies; Tanaka, Yasuko; Iniesta, Jesus
Molecules, 2009 , vol. 14, # 3 p. 1013 - 1031
