3-O-甲基-alpha-D-呋喃核糖 1,2-二乙酸酯 5-苯甲酸酯合成路线 （共 6 条）
反应条件
sulfuric acid in acetic acid
T=20°C; 24 h; Overall yield = 88 percent; Overall yield = 500 mg;
参考文献
Dou, Yan-Hui; Ding, Hai-Xin; Yang, Ru-Chun; Li, Wei; Xiao, Qiang
Chinese Chemical Letters, 2013 , vol. 24, # 5 p. 379 - 382
反应条件
1: sodium hydride / N,N-dimethyl-formamide / 0 °C
2: sulfuric acid / acetic acid / 24 h / 20 °C
View Scheme
参考文献
Dou, Yan-Hui; Ding, Hai-Xin; Yang, Ru-Chun; Li, Wei; Xiao, Qiang
Chinese Chemical Letters, 2013 , vol. 24, # 5 p. 379 - 382
反应条件
1: sodium tetrahydroborate / methanol / 3 h / 20 °C
2: sodium hydride / N,N-dimethyl-formamide / 0 °C
3: sulfuric acid / acetic acid / 24 h / 20 °C
View Scheme
参考文献
Dou, Yan-Hui; Ding, Hai-Xin; Yang, Ru-Chun; Li, Wei; Xiao, Qiang
Chinese Chemical Letters, 2013 , vol. 24, # 5 p. 379 - 382
反应条件
1: Dess-Martin periodane / dichloromethane / 5 h / 20 °C
2: sodium tetrahydroborate / methanol / 3 h / 20 °C
3: sodium hydride / N,N-dimethyl-formamide / 0 °C
4: sulfuric acid / acetic acid / 24 h / 20 °C
View Scheme
参考文献
Dou, Yan-Hui; Ding, Hai-Xin; Yang, Ru-Chun; Li, Wei; Xiao, Qiang
Chinese Chemical Letters, 2013 , vol. 24, # 5 p. 379 - 382
反应条件
1: pyridine / 4 h / 20 °C
2: Dess-Martin periodane / dichloromethane / 5 h / 20 °C
3: sodium tetrahydroborate / methanol / 3 h / 20 °C
4: sodium hydride / N,N-dimethyl-formamide / 0 °C
5: sulfuric acid / acetic acid / 24 h / 20 °C
View Scheme
参考文献
Dou, Yan-Hui; Ding, Hai-Xin; Yang, Ru-Chun; Li, Wei; Xiao, Qiang
Chinese Chemical Letters, 2013 , vol. 24, # 5 p. 379 - 382
反应条件
1: sodium carbonate; sulfuric acid / 3 h / 20 °C
2: pyridine / 4 h / 20 °C
3: Dess-Martin periodane / dichloromethane / 5 h / 20 °C
4: sodium tetrahydroborate / methanol / 3 h / 20 °C
5: sodium hydride / N,N-dimethyl-formamide / 0 °C
6: sulfuric acid / acetic acid / 24 h / 20 °C
View Scheme
参考文献
Dou, Yan-Hui; Ding, Hai-Xin; Yang, Ru-Chun; Li, Wei; Xiao, Qiang
Chinese Chemical Letters, 2013 , vol. 24, # 5 p. 379 - 382
