3-(2-苯并噻唑基)伞形酮合成路线 （共 8 条）
反应条件
1: With sodium hydroxide in ethanol; water
T=20 - 40°C;
2: With hydrogenchloride in ethanol; water
参考文献
Chao, Richard Y.; Ding, Mei-Fang; Chen, Jhao-Yu; Lee, Chuan-Chen; Lin, Shaw-Tao
Journal of the Chinese Chemical Society, 2010 , vol. 57, # 2 p. 213 - 221
反应条件
H3[PW12O40] in ethanol
T=150°C; 0.25 h; Microwave irradiation;
参考文献
Khoobi; Ramazani; Foroumadi; Hamadi; Hojjati; Shafiee
Journal of the Iranian Chemical Society, 2011 , vol. 8, # 4 p. 1036 - 1042
反应条件
sulfuric acid in water
Heating;
参考文献
Khilya; Frasinyuk; Turov
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 8 p. 1029 - 1037
反应条件
1: acetic acid / methanol / 5 h / 20 °C
2: sodium hydroxide / ethanol; water / 20 - 40 °C
View Scheme
参考文献
Chao, Richard Y.; Ding, Mei-Fang; Chen, Jhao-Yu; Lee, Chuan-Chen; Lin, Shaw-Tao
Journal of the Chinese Chemical Society, 2010 , vol. 57, # 2 p. 213 - 221
反应条件
1: piperidine / ethanol / 24 h / 20 °C
2: H2SO4 / H2O / Heating
View Scheme
参考文献
Khilya; Frasinyuk; Turov
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 8 p. 1029 - 1037
反应条件
1: piperidine / ethanol / 24 h / 20 °C
2: H2SO4 / H2O / Heating
View Scheme
参考文献
Khilya; Frasinyuk; Turov
Chemistry of Heterocyclic Compounds, 2001 , vol. 37, # 8 p. 1029 - 1037
反应条件
1: With tetrabutyl ammonium fluoride in tetrahydrofuran; N,N-dimethyl-formamide
4 h;
2: With water in tetrahydrofuran; aq. phosphate buffer; acetonitrile
pH=7; Reagent/catalystSolvent;
参考文献
Mahoney, Kaitlyn M.; Goswami, Pratik P.; Winter, Arthur H.
Journal of Organic Chemistry, 2013 , vol. 78, # 2 p. 702 - 705
反应条件
bromine
1.) DMF, water, 40 deg C, 1 h, 2.) 0 deg C, 1 h;;
参考文献
Wolfbeis, Otto S.; Koller, Ernst; Hochmuth, Petra
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 2 p. 731 - 734
