4-O-苯甲基-D-葡萄烯糖合成路线 （共 8 条）
反应条件
tetrabutyl ammonium fluoride T=20°C; Cooling with iceInert atmosphere;
参考文献
Hesek, Dusan; Lee, Mijoon; Zhang, Weilie; Noll, Bruce C.; Mobashery, Shahriar
Journal of the American Chemical Society, 2009 , vol. 131, p. 5187 - 5193
反应条件
tetrabutyl ammonium fluoride in N,N-dimethyl-formamide T=20°C; Substitution; 4 h;
参考文献
Organic Letters, , vol. 2, # 3 p. 251 - 253
反应条件
1: naH / dimethylformamide / 3 h / 20 °C 2: TBAF / dimethylformamide / 4 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 2, # 3 p. 251 - 253
反应条件
1: naH / dimethylformamide / 3 h / 20 °C 2: TBAF / dimethylformamide / 4 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 2, # 3 p. 251 - 253
反应条件
1: 70 percent / pyridine / 0 °C 2: naH / dimethylformamide / 3 h / 20 °C 3: TBAF / dimethylformamide / 4 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 2, # 3 p. 251 - 253
反应条件
1: NaH / dimethylformamide / 3 h / 20 °C 2: 484 mg / TBAF / dimethylformamide / 4 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 68, # 22 p. 8529 - 8533
反应条件
pyridine in dichloromethane T=-40°C;
参考文献
Capozzi, Giuseppe; Giannini, Sabrina; Menichetti, Stefano; Nativi, Cristina; Giolitti, Alessandro; Patacchini, Riccardo; Perrotta, Enzo; Altamura, Maria; Alberto Maggi, Carlo
Bioorganic and Medicinal Chemistry Letters, 2002 , vol. 12, # 17 p. 2263 - 2266
反应条件
1.1: (Bu3Sn)2O; mol. sieves 3 Angstroem / acetonitrile / 3 h / Heating
1.2: 89 percent / I2 / acetonitrile / 0.75 h / 20 °C
2.1: 79 percent / tetramethyl guanidinium azide / dimethylformamide / 72 h / 120 °C
View Scheme
参考文献
Kubasch, Niels; Schmidt, Richard R.
European Journal of Organic Chemistry, 2002 , # 16 p. 2710 - 2726
